Genes
The Acinetobacter baumannii (and closely related species) MLST scheme uses fragments of the following seven house-keeping genes:
- cpn60 (60-KDa chaperonin)
- fusA (elongation factor EF-G)
- gltA (citrate synthase)
- pyrG (CTP synthase)
- recA (homologous recombination factor)
- rplB (50S ribosomal protein L2)
- rpoB (RNA polymerase subunit B)
Primers for PCR amplification
cpn60:F:cpn60F ACTGTACTTGCTCAAGC
cpn60:F:cpn60R TTCAGCGATGATAAGAAGTGG
fusA:F:fusA7 ATCGGTATTTCTGCKCACATYGAT
fusA:R:fusA8 CCAACATACKYTGWACACCTTTGTT
gltA:F:gltAF AATTTACAGTGGCACATTAGGTCCC
gltA:R:gltAR GCAGAGATACCAGCAGAGATACACG
pyrG:F:pyrG7 GGTGTTGTTTCATCACTAGGWAAAGG
pyrG:R:pyrG8 ATAAATGGTAAAGAYTCGATRTCACCMA
recA:F:RA1 CCTGAATCTTCYGGTAAAAC
recA:R:RA2 GTTTCTGGGCTGCCAAACATTAC
rplB:F:rplB7 GTAGAGCGTATTGAATACGATCCTAACC
rplB:R:rplB8 CACCACCACCRTGYGGGTGATC
rpoB:F:Vic4 GGCGAAATGGC(AGT)GA(AG)AACCA (Please note: This primer sequence was corrected on Sept. 18th, 2009)
rpoB:R:Vic6 GA(AG)TC(CT)TCGAAGTTGTAACC
PCR amplification is performed at an annealing temperature of 50°C for all genes.
Primers for sequencing
We use the PCR primers for sequencing on both strands.
DNA Extraction
- Resuspend one white loop (1 µl) of 24h plate culture of bacteria in 200 µl of sterilized and free DNA water.
- Heat 10 min at 96 °C
- Centrifuge 5 min at 13000 rpm
- Pipette the supernatant and put it in 1.5 ml Eppendorf tube.
PCR amplification
- For each sample : 50 µl final volume
- Water : 34 µl 10X Buffer : 5 µl
- MgCl2 (25mM) : 3 µl
- dNTP (1.25mM each) : 4 µl
- Primer 1 (10 uM) : 1 µl
- Primer 2 (10 uM) : 1 µl
- Taq invitrogen (ref : 18038-026) 5 U/µl : 0.17 µl
- Add 2 µl of DNA (10 ng/µl) in 48 µl of mix.
- After the PCR cycle, migrate the PCR product (4µl of PCR product + 3 µl of blue) in a 1% agarose gel (100 ml of TBE 0.5X + 1g of agarose + 2 drops of BET).
Cycle
94°C 2 min
94°C 30 sec
50°C 30 sec *35
72°C 30 sec
72°C 5 min
PCR purification
- In a 96 Millipore plate (purple), put in each well 46 µl of purified PCR product and 54 µl of sterilized and free-DNA water.
- Filtration over 10 min.
- Put 50 µl of sterilized and free -DNA water in each well of the plate.
- Mix on a vortex over 10 min.
- Transfer the purified PCR product in a plate.
Sequence reaction
- Mix preparation for one reaction (one strain, one gene, one primer)
- Water : 5 µl
- 5X Buffer : 1 µl
- Primer (4µM) : 1 µl
- BigDye V1.1 : 1 µl
- Put 2 µl of purified PCR product in 8 µl of mix.
- Sequence cycling.
Sequence purification
- To each well of the plate, add 1 µl of sodium acetate 3M, 1 µl of EDTA 125 mM and 50 µl of 95 % ethanol
- Turn down the plate 10 times
- Centrifuge 30 min at 3300 rpm
- Throw out the supernatant
- Return the plate on a paper and centrifuge it 1 min at 1000 rpm
- Add 50 µl of 70 % ethanol
- Centrifuge 15 min at 3300 rpm
- Throw out the supernatant
- Return the plate on a paper and centrifuge it 1 min at 1000 rpm
- Dry the plate on the lab table over 15 min
- Conserve the plate at -20°C